Frequently Asked Questions
Here are frequently asked questions about
IBIS and UMIS. If the answer to your quesstion is not here, then please ask. You
will get a prompt reply. If you already have an instrument and want
advice or support, please see our support page.
The opinions expressed here
are offered in good faith and are based on the author's experience
in nanoindenation testing. No connection to any particular product
or instrument manufacturer is implied.
1. Why does IBIS (and UMIS) use LVDT sensors?
LVDT sensors are “linear variable differential transformers” and are
essentially inductance displacement sensors. They are inherently
linear, and have sub-nanometre resolution. Their performance is very
similar to the capacitance sensors used by other manufacturers with
one very important exception. LVDT’s are very robust. A capacitive
sensor consists of two, and sometimes three, parallel plates.
Unfortunately, the plates have to be, by necessity, of very precise
geometry, and be positioned very close together. It is common to
make these plates from glass, and very common for the plates to
break if the indenter shaft, which is connected to the centre or
moving plate, is pushed or pulled unintentionally beyond the spacing
(less than a mm) of the plates. By contrast, the LVDT sensors used
in IBIS are made from stainless steel with a titanium shaft. The
centre shaft passes right through the device and so the IBIS
nanoindentation head can withstand significant abuse by untrained or
inexperienced operators without damage. Experience over 20 years has
shown that not one single repair to these sensors has been needed.
2. What's so good about a closed loop system?
In UMIS, and IBIS, the design of the head
fetures a separate,
dedicated force sensor. The output from the force sensor is compared
to the user set-point and the difference is fed back to the pzt
actuator. This is a closed-loop system. in UMIS and IBIS, this
happens in real-time in the electronics, and is not simulated
digitally. The advantage is that the load is kept at the requested
set point no matter what the indenter is doing – this is
particularly important for creep and scratch testing. In standard
nanoindentation tests, the closed loop system ensures that repeated
tests are performed at exactly the same load increments in a precise
and repeatable manner. In some competitor systems, the situation is quite
different. One popular instrument uses the current in the coil as a
measure of the force applied to the indenter. The problem with this
system is that the current in the coil is also used to deflect the
indenter shaft support springs. The current that is used for this
deflection has to be subtracted off in order to arrive at the
residual current representing the penetration resistance of the
sample. Issues such as resistive heating of the coil also affect the
current draw. Such systems are typically calibrated by hanging
weights on the indenter shaft and measuring the residual current.
With UMIS and IBIS, the force sensor produces a signal which is
linearly proportional to the indenter load 100%, there is nothing to
subtract off. This closed loop system has been a feature of UMIS
(and now IBIS) since 1989 and the special integrator loop with feed
forward control has been designed to eliminate the possibility of
deleterious overshoot, especially as the stiffness of the system
chnages when the indenter makes contact with the surface.
3. What's the difference between a top-reference and a
surface-reference nanoindenter?
The full answer to this question has been
withdrawn due to a complaint from a competitor. One must consider that with the 10 or so various
nanoindentation instruments on the market, only two manufacturers
to the present writer's knowledge offer surface reference devices.
4. How important is calibration?
Calibration is vital, and this is where UMIS and IBIS have another
significant advantage over other instruments. UMIS was developed at
the laboratory that is responsible for the dissemination of physical
standards in Australia. The force and depth sensors with UMIS and
IBIS are separately calibrated using an extremely short validation
path to primary standards of mass and length. Competitor instruments
typically use industrial standards that are somewhat removed from
the primary standard by comparison. Worse, such instruments, with a
combined force sensor/actuator, have difficulty in establishing the
true force applied to the indenter independent of the support spring
deflection and resistive heating. Deficiencies in these types of
calibrations are often masked by the indenter area function
determination and are not noticed by the user until a sample with
mechanical properties different to that used for the area function
is tested. With UMIS and IBIS, the force and depth sensors are
independently calibrated and many years experience shows that these
sensors will retain their calibration for over 15 years and longer.
5. What about customer service? Is there a local rep I can
call upon for help?
In some cases, there is local representative for UMIS and IBIS
instruments. Even though a competitor company may offer the services
of a local representative, and provide some semblance of peace of
mind, in reality, any enquiry of substance will be forwarded to head
office and your question will be passed through several hands before
being acted upon. With Fischer-Cripps Laboratories, our agents and
customers deal direct - direct with the engineer, the programmer or
the scientist. 95% of problems can be solved by email or direct
network connection. Often problems occur when the user of the
instrument is new and needs some advice. Staff working on UMIS and
IBIS have been with the program for many years. We have a personal
commitment to our customers, many of whom have become good friends.
You don't deal with a faceless multinational company, but real
people who are interested in your problems and solutions. With
a small dedicated team, our business model is unusual compared to
most instrument companies but we are justly proud of our products
which we know will last for many years and provide quality, reliable
data. Contrary to some belief, we are able to sell direct into the
EU market at a competitive price.
6. Say I am interested, can you test a sample?
Generally yes. However, don't just send a sample without contacting
us first. We will want to know if the sample is suitable for
nanoindentation testing. Usually, a test is offered at no charge to
demonstrate the capability of the instrument. However, if the sample
is difficult, or a material that is not normally tested with this
type of instrument, a charge for time spent may be appropriate
(refunded against any future purchase).
7. How important is experience?
It's vital. It's easy for an instrument company to publish
specifications and have a product designed yesterday, but in
reality, there's a whole lot of detail needed to get it right in
nanoindentation. This attention to detail comes only at a cost - and
that is, with time. The IBIS instrument builds upon the 20 year
product history of UMIS so that it will work reliably and
consistently. Every instrument is individually calibrated, checked,
and verification tested against three standard specimens. The design
eliminates issues that plague competitor instruments. We've recently
seen some results taken with a fairly new-to-market competitor and
unfortunately, while there is a lot of marvellous gloss, the
unfortunate manufacturer, and their possible customer, have not
appreciated the instrumental issues involved in working at the nm
scale and their load-displacement curves are resplendent with subtle
but significant errors only visible to an experienced eye.
Unfortunately, these errors are easily masked by the indenter area
function until the customer comes to test a specimen with different
mechanical properties than that used for indenter calibration. With
UMIS and IBIS, real time feedback, specially designed servo loop,
low noise amplification, rigid frame, consistent robust and powerful
software, and 20 years experience etc all add up to an instrument
that works well.
8. The price you show is incredibly competitive, is this
instrument high quality?
Yes. With IBIS, the aim has been to cut down on unnecessary frills,
gadgets and custom made items and concentrate on the core capability
of nanoindentation. We can offer this level of instrumentation at
this price becuase the development costs have been recouped during
the last 20 years of the product history. This instrument will
provide results you can have confidence in. The three year warranty,
traceable calibration, the experience in instrument design, the
meticulous attention to detail, puts this instrument far ahead of
its competitors. We offer real value for money, not a cut-down cheap
product designed to attract your attention. IBIS is a quality
instrument that represents what nanoindentation should be -
reliable, accurate and affordable.